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Zhiyong Yang Zicheng Li Jinkun Zhu Qingjiang Wang Pingang He Yuzhi Fang 《Journal of separation science》2010,33(9):1312-1318
With a view of simultaneous determination of physio‐active ingredients in oolong tea infusion: sugars, amino acids, epigallocatechin gallate and ascorbic acid, a novel CZE with amperometric detection method was studied. Operated in a wall‐jet configuration, 100 mmol/L NaOH was used in detecting cell to lead the electrocatalysis oxidation behaviors of the analytes on a 300 μm diameter copper‐disc electrode (working electrode), while in separating capillary, a mild alkaline running buffer consisting in a mixture of 30 mmol/L borate and 40 mmol/L phosphates charged and carried analytes to detecting end. The methodology research was performed for system stability and suitability. Under the optimal CE conditions, analytes could be separated within moderate time period. Good linearity between peak area and concentration existed over three orders of magnitude; lower RSD and LOD were achieved. The oolong tea infusion was assayed and result was satisfactory. 相似文献
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在任意实的Banach空间中研究了用具误差的修正的Ishikawa与Mann迭代程序来逼近一致L-Lipschitz的渐近伪压缩映象不动点的强收敛性问题,在去掉条件$$\sum\limits_{n=0}^{\infty}\alpha_{n}^{2}<\infty, \q \sum\limits_{n=0}^{\infty }\gamma_{n}<\infty,\q \sum\limits_{n=0}^{\infty }\alpha_{n}(\beta_{n}+\delta_{n})<\infty,\q \sum\limits_{n=0}^{\infty}\alpha_{n}(k_{n}-1)<\infty$$之下,证明了相关文献的结果仍然成立.所得结果不但改进和推广了最近一些人的最新结果,而且也从根本上改进了定理的证明方法. 相似文献
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The paper focuses on solving a common and important problem of NIR quantitative analysis in multi-component systems: how to significantly reduce the size of the calibration set while not impairing the predictive precision. To cope with the problem orthogonal discrete wavelet packet transform (WPT), the least correlation design and correlation coefficient test (r-test) have been combined together. As three examples, a two-component carbon tetrachloride system with 21 calibration samples, a two-component aqueous system with 21 calibration samples, and a two-component aqueous system with 41 calibration samples have been treated with the proposed strategy, respectively. In comparison with some previous methods based on much more calibration samples, the results out of the strategy showed that the predictive ability was not obviously decreased for the first system while being clearly strengthened for the second one, and the predictive precision out of the third one was even satisfactory enough for most cases of quantitative analysis. In addition, all important factors and parameters related to our strategy are discussed in detail. 相似文献
46.
This paper examines the universal quantitative properties of the fractional- and integer-order Chen?CLee systems. A?series of bifurcation diagrams of the system were generated in order to measure Feigenbaum??s constants. It was found that the measured values of the integer-order system were accurately approaching their universal constants, while the errors between measured values of the fractional-order system and the universal constants were not very large. The results showed that both the fractional- and integer-order Chen?CLee systems belonged to a quadratic map. To the authors?? knowledge, this is the first paper to measure Feigenbaum??s constants in fractional-order systems. 相似文献
47.
本文研究了一致凸Banach空间中渐近拟非扩展型映象和渐近非扩展型映象T的不动点的迭代逼近问题.利用范数不等式,在去掉[3]中一个较强条件的情况下,证明了T的具误差的Ishikawa迭代序列中收敛于T的某个不动点.所得定理推广和改进了已有的部分结果。 相似文献
48.
本文在去掉条件“‖Tnxn-xn‖→0(n→∞)”的情况下,在任意实的Banach空间中研究了用具误差的修正的Ishikawa与Mann迭代程序来逼近非Lipschitz的渐近伪压缩映象不动点的强收敛性问题;所得结果不但改进和推广了张石生教授与曾六川教授的结果,而且也从根本上改进了定理的证明方法. 相似文献
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Yusheng Fu Haiyan Tan Xiujian Wu Xiaohe Wu Yongzheng Yang Yanling Gao Ruowei Liu Min Qi Xiaoyun Chen Yaochao Ning Weidong Sun Nianhuan Chang Junjie Ma Kang Cheng Hongni Yang Qing Li Ping Wang Chaoran Wu Hong Xian Li Wang 《Electrophoresis》2021,42(9-10):1043-1049
Currently, the global healthcare market is increasing at high speed with the impendent global aging issue. Healthcare Industry 4.0 has emerged as an efficient solution towards the aging issue since it was integrated with ubiquitous medical sensors, big health processing platform, high bandwidth, speed technologies, and medical services, etc. It is believed to fulfil the requirement of the tremendously growing health market. The acquisition of medical data acts as the dominant precondition to implement the Healthcare Industry 4.0. In the same way, the widely available smartphone could serve as the best biomedical information collect station. In this study, a smartphone-powered photochemical dongle is demonstrated to precisely estimate blood creatinine from the fingertip blood, which works as a highly compact reflectance spectral analyzer with an enzymatically dry chemical test strip. Comparing with conventional laboratory facility for the evaluation and treatment of chronic kidney disease (CKD), it implemented the platform of point care with agreed accuracy. In order to estimate the efficiency of treatment and recovery of the CKD, the proposed photochemical dongle would provide a flexible and rapid platform for point of care. Furthermore, the proposed measured technology is very promising method for remote CKD management. 相似文献